Research Article

Development and Validation of Analytical Procedure for Elemental Impurities in Rosuvastatin Calcium Tablets by ICP-MS and Microwave Digestion

Table 6

Results of linearity, range, and LOQ.

ElementRangeEquationsLOQ (µg L−1)

111Cd0∼2.5 µg·L−1f (x) = 9292.8026x + 11.33080.99960.25
208Pb0∼2.5 µg·L−1f (x) = 177518.3179x + 7591.98061.00000.25
75As0∼7.5 µg·L−1f (x) = 2139.7435x + 6.99350.99990.75
202Hg0∼15 µg·L−1f (x) = 34197.1263x + 688.04500.99991.5
59Co0∼25 µg·L−1f (x) = 45810.3360x + 241.28380.99992.5
51V0∼50 µg·L−1f (x) = 14661.8418x + 64.36820.99995.0
60Ni0∼100 µg·L−1f (x) = 13025.5736x + 3519.17960.999810